Species

Vivianite

Vivianite is a hydrated iron phosphate, hardness 1.5 to 2, colourless when fresh and darkening to indigo and black. Cornish type locality and Bolivian crystals.

Formula Fe3(PO4)2 8H2OHardness 1.5 to 2Density 2.68Type locality St Agnes, CornwallNamed for John Henry Vivian

Vivianite is a hydrated iron phosphate, hardness 1.5 to 2, described in 1817 and named for John Henry Vivian (1785-1855), who found it in Cornwall. Fresh material is colourless to pale green; oxidation turns it blue, then indigo, then black. Prismatic crystals reach 1.3 m.

In short

  • The colour is the damage. The deep indigo that makes vivianite famous is an oxidation product. Genuinely fresh vivianite is nearly colourless, and every specimen you see is already partway through the change.
  • It is very soft and it bends. Hardness 1.5 to 2, perfect cleavage on {010}, and flexible, sectile crystals — you can cut it with a knife and it will deform rather than snap.
  • The type locality is British: Cornwall, at St Agnes, with other material from mines in St Just and Kea. Almost nobody associates the species with Cornwall, and the label does.
  • The best crystallised specimens are Bolivian, from Llallagua and the other tin districts, with huge crystals also from Anloua in Cameroon.
  • It forms in the oxidised zone of metallic ore deposits and in granite pegmatites, but also in bog iron ores, peat, lake sediments and replacing organic material in fossil bone.
How vivianite changes, and what it means for a specimen
StateColourWhat has happenedWhat to do
Fresh, unexposedColourless to very pale greenIron still in the ferrous stateSeal it dark immediately. This state does not survive display
Early oxidationBlue to dark greenish bluePartial oxidation to ferric ironThe state most collectors want. Stabilise by storing dark and dry
AdvancedIndigo to dark blue, strongly pleochroicFurther oxidation through the crystalStill a fine specimen. Handle minimally
TerminalBrown, purplish black, black; streak brownOxidation essentially complete; crystals often crumblingNot recoverable. Photograph and keep the label

A Cornish type locality nobody expects

Vivianite is named for John Henry Vivian, 1785 to 1855, the Welsh-Cornish mineralogist of Truro who discovered the species, and it was described in 1817. The Handbook of Mineralogy gives the English occurrences as St Agnes and other mines in St Just and Kea, Cornwall, with the type material from the St Agnes district.

This is worth knowing for a specific practical reason: it is one of the small number of species with a British type locality that collectors do not associate with Britain at all. Cornish vivianite is scarce, it is old — the mines were finished long ago, as our Cornwall page sets out — and it is not what anyone means when they say vivianite. That combination is exactly the one where a well-documented old label carries disproportionate weight, and where an under-described piece in a mixed lot occasionally turns out to be significant. Our notes on old labels cover what makes such a label checkable.

Do not, however, expect Cornish material to look like the Bolivian crystals in photographs. It does not. British vivianite is generally small, often earthy or crusty, and its interest is historical rather than aesthetic.

The colour, and why it is a clock

Vivianite is one of the clearest examples in mineralogy of a species whose famous appearance is a state of decay. Freshly exposed material is transparent and colourless to very pale green. On exposure the ferrous iron oxidises, and the crystal runs through dark blue, dark greenish blue and indigo, then to brown, purplish black and finally black. The streak follows: white at first, altering to dark blue and then brown.

Two consequences for a collector. First, a colourless vivianite is a very recent one, and it will not stay colourless. Second, the process does not stop where you would like it to. The rich indigo that people buy is a waypoint, not an end state, and the specimen continues to darken in a cabinet, slowly, indefinitely.

What you can do is slow it. Store the specimen sealed and dry, keep it dark, and handle it as little as possible — the same regime as for the genuinely light-sensitive species on our page about minerals that fade in light, applied here to an oxidation rather than a photochemical reaction. What you cannot do is reverse it. There is no treatment that puts a black vivianite back to blue, and any specimen offered as unusually bright should prompt the same questions as any other suspiciously good colour.

The pleochroism is worth seeing while you have the chance: in transmitted light the crystal is deep blue in one direction and pale yellowish or bluish green in the others, which is unusually strong for a common mineral and is diagnostic.

Softness, cleavage and handling

At hardness 1.5 to 2, vivianite is softer than a fingernail is hard in the wrong direction, and it has perfect cleavage on {010}. The tenacity is the unusual part: it is flexible and sectile, so a thin cleavage plate bends rather than shattering and a blade cuts it. That makes it one of the very few minerals that a careless thumb can permanently deform rather than merely chip.

Handling rules that follow, and they are stricter than for most species:

  • Support it under the matrix. Never grip a crystal.
  • Store it in its own rigid box, with nothing else in the box. Anything harder — which is nearly everything — will mark it.
  • Do not clean it. Water, ultrasonic baths and brushes are all worse than the dust.
  • If it must be shipped, it is in the softest class on our page about packing and shipping specimens: tissue and cut foam, nothing touching the crystals, double boxed.

Where the great crystals come from

The species is widespread — it turns up in bog iron ore, in peat, in lake sediment, and famously replacing organic material in fossil bone, which is why palaeontologists know it as well as mineralogists do. Well-crystallised material is another matter.

Bolivia is the standard, with exceptional examples from Llallagua, Poopó, Avicaya, Tazna, Monserrat, Morococala and Tatasi — the tin and silver districts of the Altiplano. Huge crystals come from Anloua, near Ngaoundéré in Cameroon; the largest recorded prismatic crystals of the species reach 1.3 m. Other significant localities are Hagendorf in Bavaria, the Stari Trg mine at Trepča in Serbia — which is also a fine pyrrhotite locality — the Taman Peninsula in Russia, Kerch in Crimea, the Énio pegmatite near Galiléia in Minas Gerais, Santa Eulalia in Chihuahua, and several American occurrences including the Blackbird mine in Idaho and the Foote mine in North Carolina.

When buying, the questions that matter are about storage rather than about the mineral: how long has it been out of the ground, how has it been kept, and has anything been done to the colour. A seller who can answer the first two has usually taken care of the third. If a good crystallised vivianite with a real locality is what you want, put it on the wanted list — we hold no stock, and on a species this fragile the value in having somebody look first is unusually high.

Questions

Why did my vivianite turn black?
Oxidation. Vivianite is a ferrous iron phosphate, and on exposure the iron oxidises, taking the crystal from colourless or pale green through blue and indigo to brown and finally black — the Handbook of Mineralogy records exactly that sequence, with the streak altering from white to dark blue and brown. It cannot be reversed; storing the specimen sealed, dry and dark slows it.
Is vivianite really from Cornwall?
The type locality is Cornish — St Agnes, with other English material from mines in St Just and Kea — and the species is named for John Henry Vivian of Truro, who discovered it. Cornish material is scarce and generally unimpressive next to Bolivian crystals; its value is historical and depends heavily on the label.
How should I store vivianite?
Sealed, dry, dark, and alone. Its own rigid box with nothing else in it, because at hardness 1.5 to 2 with perfect cleavage almost any other specimen will mark it. Keep handling to a minimum, support it under the matrix rather than by a crystal, and do not attempt to clean it.
Can vivianite be cleaned?
Effectively no. It is soft, perfectly cleavable, flexible and water-sensitive in the sense that moisture accelerates the oxidation you are trying to slow. Ultrasonic cleaning will destroy it. Dust removal with a very soft brush, done rarely, is the limit.
What is vivianite in fossil bone?
The same mineral, formed where phosphate from bone and iron from groundwater meet under reducing conditions. It appears as blue crusts and small crystals on and inside fossil and sub-fossil bone, and it is common enough in bog and lake settings that palaeontological conservators deal with it routinely.